Luhede, Laura
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Item-typ:Veröffentlichung, Formulation and Rheological Characterization of Premix EmulsificationFormulation and Rheological Characterization of Premix EmulsificationWissenschaftlicher ArtikelBand:87Heft:8120 107 - Some of the metrics are blocked by yourconsent settings
Item-typ:Veröffentlichung, Premix membrane emulsification using flat microfiltration inorganic membranes with tailored structure and composition(Elsevier, 2020-04-20); ; ; ; Uniform oil-in-water emulsions were prepared using MCT (medium-chain fatty acid triglyceride, 10 wt%) as the oily dispersed phase and polysorbate 80 as the surfactant (1 wt%). The emulsification process was performed via premix membrane emulsification (PME) using 3 flat microfiltration ceramic membranes with different mean pore sizes (dm): borosilicate (symmetric, commercial, dm: 1.39 μm); SiOC (symmetric, manufactured, dm: 1.76 μm); and mullite (asymmetric, manufactured, dm: 1.18 μm). The droplets size and their distribution varied according to the membrane type and number of permeation cycles (up to a limit of 2 passes). All prepared emulsions presented a tendency to monomodal droplet distribution with span values in the range of 0.82–0.97. The coarse emulsion (premix) droplets were reduced from 6.30 to 4.50–2.17 μm. The asymmetric membrane (mullite) exhibited the highest permeation fluxes at constant relative pressure for both water (43.1 × 10−3 m3 m−2 s−1) and premix (Pass 1: 4.6 × 10−3 m3 m−2 s−1; Pass 2: 5.3 × 10−3 m3 m−2 s−1), still maintaining satisfactory emulsification results.Wissenschaftlicher Artikel132 123 - Some of the metrics are blocked by yourconsent settings
Item-typ:Veröffentlichung, Stability of multiple emulsions under shear stressMultiple liquid emulsions of the water in oil in water (W1/O/W2) type are used in a variety of consumer or technical applications, for instance in the encapsulation of certain active ingredients. The encapsulation process and release mechanisms of the inner phase of the carrier drops are important in order to properly process and formulate such liquid-liquid systems. In this work the stability and breakage of multiple W1/O/W2 emulsions under mechanical shear stress are investigated for emulsions with different surfactants and surfactant concentrations of the internal emulsion. Stressing the emulsions in a mechanical stirring process is compared to the membrane emulsification process. The membrane emulsification process results in higher encapsulation efficiencies than the stirring process. The emulsion droplets were subjected to shear stress below and above the critical capillary number for drop breakup. The results show that stable inner emulsions with sufficient surfactant concentrations increase the overall encapsulation efficiency for multiple emulsions subjected to shear stress, although the effect is not prominent. The depletion of the carrier oil droplets could be achieved for Ca numbers below the critical limit, reducing the encapsulation efficiency below 10 %. This shows that even a low shear stress can result in content release from the internal droplet phase. The experimental emulsion release study is supported by a numerical simulation of drop deformation and break-up under shear stress.Wissenschaftlicher ArtikelBand:98Heft:1105 147